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id="content_box-1639805533587-0" class="d_gridCell_0 p_gridCell"><div class="rnn75jx" id="c_new_detail_011-1639816997710"> <div id="55pv5zb" class="e_container-2 s_layout"> <div id="vnhbhjj" class="cbox-2-0 p_item"><div id="tpvz5br" class="e_container-12 s_layout"> <div id="5hl5hjl" class="cbox-12-0 p_item"><div id="hd55lzr" class="e_container-19 s_layout"> <div id="xn55ffx" class="cbox-19-0 p_item"><h1 class="e_h1-20 s_subtitle"> 聚氯三氟乙烯的制作方法是什么 </h1><div id="nvpjdd5" class="e_container-13 s_layout"> <div id="j5jbf5v" class="cbox-13-0 p_item"><P class="e_timeFormat-14 s_title">2021-07-13</P></div> </div></div> </div></div> </div><hr class="e_line-26 s_line" /><div id="7dxr5j5" class="e_richText-24 s_title"> <p>聚<strong>氯三氟乙烯</strong>是開(kāi)發(fā)和生產(chǎn)的熱塑性氟塑料。1937年法國公司發(fā)表了第一份制備報告，后來(lái)在曼哈頓項目的過(guò)程中，美國對其制備工藝路線(xiàn)和產(chǎn)品性能做了大量的研究工作，由3M公司于1942年投產(chǎn)，并以Kel-F商標銷(xiāo)售。1959年，我國開(kāi)始研制PCTFE樹(shù)脂。1960年，試驗成功。1966年建成年產(chǎn)25噸PCTFE樹(shù)脂的生產(chǎn)裝置。</p><p style="text-align: center;"><img src="https://omo-oss-image.thefastimg.com/portal-saas/new2023041118021774750/cms/image/16c8c9a0-4174-4e5f-a751-cc70e114af94.jpg" alt="聚氯三氟乙烯的制作方法是什么" width="294" height="235" border="0" vspace="0" title="聚氯三氟乙烯的制作方法是什么" style="width: 294px; height: 235px;"/></p><p>聚<strong>氯三氟乙烯</strong>是三氟氯乙烯的均聚物，其結構是在主碳鏈周?chē)蟹吐仍印?/p><p> 聚氯三氟乙烯化學(xué)結構通式如下：</p><p> 聚氯三氟乙烯的分子結構中的F原子使聚合物具有化學(xué)惰性，而CI原子使聚合物具有透明性、熱塑性和硬度。因此，pcife是一種高穩定性、耐熱性、不燃性、不吸濕性、透氣性和惰性的優(yōu)質(zhì)熱塑性樹(shù)脂。由于PCTFE分子結構中存在C-CI鍵，PCTFE的硬度、剛度、抗蠕變性、滲透性、熔點(diǎn)和熔體粘度均優(yōu)于聚四氟乙烯和聚四氟乙烯六氟丙烯（FEP），但耐熱性和化學(xué)惰性比PTFE和FEP稍差。</p><p> 聚<strong>氯三氟乙烯</strong>的熔化溫度213℃，具有優(yōu)異的化學(xué)穩定性、絕緣性和耐候性，可在-196-125℃下長(cháng)期使用，機械強度和硬度均優(yōu)于聚四氟乙烯，薄膜具有較好的透明性和較低的透氣性。PCTFE是一種結晶聚合物，熔點(diǎn)為218.33℃，密度為2.13g/cm3（g/cm3）。</p><p> PCTFE是由具有重復CF（CL）-CF單元的線(xiàn)性主鏈的三氟氯乙烯自由基引發(fā)聚合的產(chǎn)物。</p><p> 聚氯三氟乙烯在室溫下對大多數活性化學(xué)物質(zhì)都是惰性的，但在212t以上的少數溶劑中能溶解，也能被某些溶劑特別是氯化溶劑溶脹。PCTFE具有良好的氣體阻隔能力，其透濕性是所有透明塑料薄膜中較低的。其電學(xué)性能與其它全氟聚合物相似，但介電常數和損耗因子稍高，特別是在高頻下。PCTFE可以制作厚（1/8英寸）的光學(xué)透明部件。</p><p> 聚氯三氟乙烯主要通過(guò)懸浮聚合、乳液聚合等方法制備。</p><p> 1、懸浮聚合</p><p> 該方法用于制備高分子量聚三氟乙烯。向聚合釜中加入水、引發(fā)劑過(guò)硫酸銨、還原劑焦亞硫酸鈉和pH緩沖液，再加入三氟氯乙烯進(jìn)行懸浮聚合。</p><p> 2、乳液聚合</p><p> 三氟氯乙烯100份，水30份，引發(fā)劑2過(guò)硫酸鉀2.4份，乳化劑全氟辛酸2.4份，調至pH7，30℃聚合20h，得到粒徑為0.1um的穩定的聚氟乙烯-氯乙烯乳液。中國的主要制造商是上海曙光化工廠(chǎng)。</p> </div><hr class="e_line-27 s_line" /><div id="tnfzfv5" class="e_container-29 s_layout"> <div id="bd5fxlb" class="cbox-29-0 p_item"><div id="5txfndp" class="e_container-30 s_layout"> <div id="vlr55j5" class="cbox-30-0 p_item"><p class="e_text-59 s_body"> 上一條 </p></div> <div id="xx5j5bb" class="cbox-30-1 p_item"><p class="e_text-58 s_title"> <a href="/news/33.html" target="_self"> 氯三氟乙烯的性能是什么 </a> </p></div> </div></div> <div id="pd5d55h" class="cbox-29-1 p_item"><div id="f5pjz5h" class="e_container-55 s_layout"> <div id="55vb5xj" 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